HomeMy WebLinkAboutSoil Sample from GDC Building on Barber StEMPIRE ENGINEERING & TESTING INC.
P.O. Box 776
Vero Beach, Florida 32961
January 15, 1992
City of Sebastian
Post Office Box 127
Sebastian, Florida 32978
Attention: Mr. Dan Eckis
Reference: GDC Building
Barber Street
Sebastian, FL.
Dear Dan,
50 Fifth Court
Vero Beach, Florida 32962
As you requested, a composite soil sample was taken from the
above referenced site and analyzed for Volatile Organic
Compound (VOC) pursuant to EPA Method 610/602 and Polynuclear
Aromatic Hydrocarbons (PAH) according to EPA Method 610.
SOIL SAMPLING
A composite soil sample was taken using a stainless steel
hand auger from 0-6'. The samples were placed in appropriate
containers, stored in an iced cooler and transported to
Orlando Laboratories, Inc., in Orlando, Florida.
The sample was taken adjacent to the guard rail which was
used to project two above ground fuel tanks which have been
removed.
RESULTS
Attached are the results from Orlando Laboratories. The
samples are all clean, with nothing detected.
If you have any question, or if we can be of further
assistance, please call this office.
Respectfully,
EMPI ENGINEERING AND TESTING, INC.
a ry 0. Wagn .E.
Preside t/Consulting Engineer
VERO BEACH (407) 569-0153
FAX (407) 569-3360
obert ?.ZWalker
Project Coordinator
ST. LUCIE (407) 337-7911
MELBOURNE (407) 676-9956
ORLANDO LABORATORIES
P.O. BOX 149127.ORLANDO, FLORIDA 32814
I4� (407) 896-6646 • FAX: (407) 898-6588
67676
INVOICE TO: REPORT TO:
EMPIRE ENGINEERING & TESTING EMPIRE ENGINEERING & TESTING
50 STH COURT 50 5TH COURT
VERO BEACH, FL 32962 VERO BEACH, FL 32962
BOB WALKER BOB WALKER
INVOICE DATE CUSTOMER P.O. / CONTRACT NO. LAB WORK ORDER NUMBER
01/13/92 91-12-428
QTY. ANALYTICAL LABORATORY SERVICES UNIT PRICE TOTALAMOUNT
CLIENT WORK ID: SEBASTIAN GDC BLDG.
1 JOB 8182S
COMBINED EPA 8010 & 8020
145.00
145.00
1 81008
POLYNUCLEAR AROMATIC\SOIL
145.00
145.00
1 S PREP
SOIL PREP FEE
25.00
25.00
TOTAL INVOICE AMOUNT $315.00
Thank you for choosing Orlando Laboratories, Inc. A Finance Charge of 1 % per month
will be added on past due amount after 60 days.
ORLANDO LABORATORIES
P.O. BOX 149127 • ORLANDO, FLORIDA 32814
(407) 896-6646 • FAX: (407) 898-6588
REPORT OF ANALYSIS
Empire Engineering & Testing
50 5th Court
Vero Beach, FL 32962
Attn: Bob Walker
Work ID: Sebastian GDC Bldg.
Samples collected by: Client
Total Samples: 3
SAMPLE IDENTIFICATION
01 Seb GDC
02 Seb GDC
03 Method Blank
Work Order # :
Date Received:
Date Reported:
OLI Contact:
TEST CODES and NAMES used on this report
80105 Purgeable Halocarbon\Soil
8020S Purgeable Aromatics\Soil
81005 Polynuclear Aromatic\Soil
91-12-428
12/30/91
01/10/92
J_BEATO
OLI Florida Department of Health & Rehabilitative Service Identification Numbers are:
Drinking Water Certification Number 83141, Environmental Certification Number E83033
Respectful} SulAitted,
I John Hobbs "
LABORATORY DIRECTOR
Eric Malarek
QUALITY CONTROL
ORLANDO LABORATORIES,INC.
Received: 12/30/91
REPORT OF ANALYSIS
Results by Sample
Page 2
Work Order # 91-12-428
SAMPLE ID
Seb GDC
SAMPLE#
01A
DATE COLLECTED
12/26/91 09:30:00 _
MATRIX
SOIL
TEST NAME
Purgeable Halocarbon\Soil
TEST CODE
8010S
SAMPLE TYPE
SOIL
DATE EXTRACTED
NA
UNITS
ug/kq
DATE RUN
01/06/92
ANALYST
SRK
DILUTION FACTOR
5
METHOD
8010
X MOISTURE
12.7
RESULT/QUALIFIER
Chloromethane
6
U
Bromomethane
_ 6
U
Vinyl chloride
_� 6
U
Dichlorodifluoromethane
6
U
Chloroethane
6
U
Methylene Chloride
6
U
1,1-Dichloroethene
6
U
Trichlorofluoromethane
_ 6
U
1,1-Dichloroethane
6
U
t-1,2-Dichloroethene
6
U
Chloroform
6
U
1,2-Dichloroethane
" 6
U
1,1,1 -Trichloroethane
6
U
Carbon tetrachloride
_ 6
U
Bromodichloromethane
_ 6
U
1,2-Dichloropropane
6
U
t-1,3-Oichloropr-opene
6
U
Trichloroethene
6
U
Dibromochloromethane
6
U
1,1,2 -Trichloroethane
6
U
c-1,3-0ichIoropropene
_ _ 6_U
2-Chloroethylvinylether
_ 6
U
Bromoform
_ 6
U
1,1,2,2 -Tetrachloroethane
6
U
Tetrachloroethene
_ 6
U
1,2-Dibromo-3-chloropropane
_ 6
U
1,2 -Dichlorobenzene
6
U
1,3 -Dichlorobenzene
6
U
1,4 -Dichlorobenzene
i 6
U
Chlorobenzene
6
U
Elevated detection limits caused by dilution of sample. Dilution was necessary
because of matrix interference.
ORLANDO LABORATORIES,INC. REPORT OF ANALYSIS
Received: 12/30/91 Results by Sample
SAMPLE ID Seb GDC
DATE COLLECTED 12/26/91 09:30:00
TEST NAME Purgeable Aromatics\Soil
SAMPLE TYPE SOIL
UNITS UG/KG
ANALYST SRK
METHOD 8020
Page 3
Work Order
RESULT/QUALIFIER
Benzene
6
U
Toluene
6
U
Chlorobenzene
6
U
Ethylbenzene
6
U
Styrene
6
U
Total Xylenes
_ 6
U
1,2 -Dichlorobenzene
6.0
1,3 -Dichlorobenzene
_ 6
U
1,4 -Dichlorobenzene.
6
U
MTBE
6
U
Page 3
Work Order
# 91-12-428
SAMPLE#
01A
MATRIX
SOIL
TEST CODE
8020S
DATE EXTRACTED NA
DATE RUN 01/06/92
DILUTION FACTOR 5
MOISTURE 12.7
Elevated detection limits caused by dilution of sample. Dilution was necessary
because of matrix interference.
Page 4
ORLANDO LABORATORIES,INC. REPORT
OF ANALYSIS
Work Order # 91-12-428
Received: 12/30/91
Results
by Sample
SAMPLE ID
Seb GDC
SAMPLE#
02A
DATE COLLECTED
12/26/91
09:30:00_
MATRIX
SOIL
TEST NAME
Polynuclear Aromatic\Soil
TEST CODE
8100S
SAMPLE TYPE
SOIL
DATE EXTRACTED
01/02/92
UNITS
uq/kq
DATE RUN
01/05/92
ANALYST
RJW
DILUTION FACTOR
1
Method:
8100
% MOISTURE
12.7
RESULT/QUALIFIER*
Naphthalene
380
U
Acenaphthylene
i_ 380_
U
Acenaphthene
380
U
Fluorene
J 380
U
Phenanthrene
380
U
Anthracene
380_
U
Fluoranthene
_ 380_
U
Pyrene
380
U
Benzo(a)anthracene
_ 380
U_
Chrysene
J_ 380_
U
Benzo(b)fluoranthene
_ 380
U
Benzo (k) f I uoranthene
_. 380 _
U
Benzo(a)pyrene
^. 380
U
Indeno(1,2,3-cd)pyrene
380
U
Dibenzo(a,h)anthracene
_ 380w
U
Benzo(g,h,i)perylene
380_
U
1 -Methylnaphthalene
380
U
2 -Methylnaphthalene
__ 380
U
Page 5
ORLANDO LABORATORIES,INC. REPORT OF ANALYSIS Work Order f 91-12-428
Received: 12/30/91 Results by Sample
SAMPLE ID Method Blank
DATE COLLECTED not specified
TEST NAME Purgeable Halocarbon\Soil
SAMPLE TYPE SOIL
UNITS ug/kq
ANALYST SRK
METHOD 8010
SAMPLED 03A
MATRIX METHOD
TEST CODE 80105
DATE EXTRACTED NA
DATE RUN 01/06/92
DILUTION FACTOR 1
MOISTURE 0
RESULT/QUALIFIER
Chloromethane
_ 1.0
U
Bromomethane
1.0
U
Vinyl chloride
1.0~U
Dichlorodifluoromethane
_ 1.0
U
Chloroethane
_ 1.0
U
Methylene Chloride
1.0
U
1,1-Dichloroethene
i 1.0
U
Trichlorofluoromethane
1.0
U
1,1-Dichloroethane
�. 1.0
U
t-1,2-Dichloroethene
�.,. 1.0_U
Ch I oroforrn
_ 1.0
U
1,2-Dichloroethane
1.0
U
1,1,1 -Trichloroethane
_ 1.0
U
Carbon tetrachloride
1.0
U
Bromodichloromethane
1.0
U
1,2-Dichloropropane
1.0
U
t-1,3-Dichloropropene
_. 1.0
U
Trichloroethene
1.0
U
Dibromochloromethane
_! 1.0
U
1,1,2 -Trichloroethane
l 1.0
U
c-1,3-Dichloropropene
i 1.0
U
2-Chloroethylvinylether
_ 1.0
U
Bromoform
_ 1.0
U
1,1,2,2-Teti-achloroethane
i 1.0
U
Tetrachloroethene
1.0
U
1,2-Dibromo-3-chloropropane
1.0
U
1,2 -Dichlorobenzene
1.0
U
1,3 -Dichlorobenzene
1.0
U
1,4 -Dichlorobenzene
1.0
U
Chlorobenzene
1.0
U
SAMPLED 03A
MATRIX METHOD
TEST CODE 80105
DATE EXTRACTED NA
DATE RUN 01/06/92
DILUTION FACTOR 1
MOISTURE 0
ORLANDO LABORATORIES,INC.
Received: 12/30/91
SAMPLE ID Method Blank
DATE COLLECTED not specified
TEST NAME Purgeable Aromatics\Soil
SAMPLE TYPE SOIL
UNITS UG/KG
ANALYST SRK
METHOD 8020
REPORT OF ANALYSIS
Results by Sample
Page 6
Work Order f 91-12-428
SAMPLE# 03A
MATRIX METHOD
TEST CODE 8020S
DATE EXTRACTED NA
DATE RUN 01/06/92
DILUTION FACTOR 1
X MOISTURE 0
ANK
RESULT/QUALIFIER
Benzene
1.0
U
Toluene
1.0
U
Chlorobenzene
_ 1.0
U
Ethylbenzene
1.0
U
Styrene
_ 1.0_.0
Total Xylenes
i 1.0
U
1,2 -Dichlorobenzene
1.0
U
1,3 -Dichlorobenzene
1.0
U
1,4 -Dichlorobenzene
— 1.0
U
MTBE
1.0
U
Page 6
Work Order f 91-12-428
SAMPLE# 03A
MATRIX METHOD
TEST CODE 8020S
DATE EXTRACTED NA
DATE RUN 01/06/92
DILUTION FACTOR 1
X MOISTURE 0
ANK
ORLANDO LABORATORIES,INC. REPORT OF ANALYSIS
Received: 12/30/91 Results by Sample
SAMPLE ID Method Blank
DATE COLLECTED not specified _
TEST NAME Polynuclear Aromatic\Soil
SAMPLE TYPE
SOIL
UNITS
ug/kq
ANALYST
RJW
Method:
8100
RESULT/QUALIFIER+,
Naphthalene
330
U
Acenaphthylene
330_
U
Acenaphthene
330
U
Fluorene
330
U
Phenanthrene
330_-
U
Anthracene
330
U
Fluoranthene
330
U
Pyrene
330_
U
Benzo(a)anthracene
_ 330
U
Chrysene
_ 330
U
Benzo(b)fluoranthene
�_- 330-
U
Benzo(k)fluoranthene
330
U
Benzo(a)pyrene
— 330^
U
Indeno(1,2,3-cd)pyrene
— 330
U
Dibenzo(a,h)anthracene
330
U
Benzo(g,h,i)perylene
330
U
1 -Methylnaphthalene
330
U
2 -Methylnaphthalene
_ 330_
U
Page 7
Work Order- f 91-12-428
SAMPLEf 03A
MATRIX METHOD BLANK'
TEST CODE 8100S
DATE EXTRACTED 01/02/92
DATE RUN 01/03/92
DILUTION FACTOR 1
MOISTURE 0
Page 8
ORLANDO LABORATDRIES,INC- REPORT OF ANALYSIS Work Order 0 91-12-428
Received: 12B0/91 NonReported Work
FRACTION AND TEST CODES FOR WORK NOT REPORTED ELSEWHERE
Page 9
ORLANDO LABORATORIES INC.
GC ORGANICS
MATRIX SPIKE RESULTS
MATRIX : SOIL/SEDIMENT/SOLIDS LAB SAMPLE # 9107078-03
REPORT DATE : 01-07-1992 ANALYSIS DATE 01/06/92
COMMENTS :
MATRIX SPIKE OUALITY CONTROL LIMITS
WATER SOIL
LOWER UPPER RPD LOWER UPPER RPD
TOLUENE 81 118 17 80 144 52
CHLOROBENZENE 78 123 12 I 91 116 29
ETHYLBENZENE 80 115 15 y 55 145 44 f
AMOUNT
SAMPLE
MS
MS %
MSD
MSD%
COMPOUND
SPIKED
RESULT
RESULT
RECOVERY
RESULT
RECOVERY
RPD
TOLUENE
100
0
100
100
105
105
5
CHLOROBENZENE
100
0
96
96
103
103
7
ETHYLBENZENE
100
0
98
98
103
103
5
COMMENTS :
MATRIX SPIKE OUALITY CONTROL LIMITS
WATER SOIL
LOWER UPPER RPD LOWER UPPER RPD
TOLUENE 81 118 17 80 144 52
CHLOROBENZENE 78 123 12 I 91 116 29
ETHYLBENZENE 80 115 15 y 55 145 44 f
ORLANDO LABORATORIES INC.
GC ORGANICS
MATRIX SPIKE RESULTS
MATRIX : SOIL/SEDIMENT/SOLIDS
REPORT DATE : 01-07-1992
Page 10
LAB SAMPLE I : 9107078-03
ANALYSIS DATE : 01/06/92
MATRIX SPIKE QUALITY CONTROL LIMITS
AMOUNT
SAMPLE
MS
MS %
MSD
MSD%
1,1-Dichloroethane
COMPOUND
SPIKED
RESULT
RESULT
RECOVERY
RESULT
RECOVERY
RPD
138
29
41
138
15
1,1,2,2 -Tetrachloroethane
60
144
1,1-Dichloroethane
50
0
61
122
76
152
22
1,1,1 -Trichloroethane
50
0
56
112
67
134
18
1,1,2,2 -Tetrachloroethane
50
0
46
92
51
102
10
MATRIX SPIKE QUALITY CONTROL LIMITS
NOTE: * Parameter outside of QC limits due to matrix effects.
LOWER
WATER
UPPER
RPD
LOWER
SOIL
UPPER
RPD
1,1-Dichloroethane
65
139
27
46
176
27
1,1,1 -Trichloroethane
68
138
29
41
138
15
1,1,2,2 -Tetrachloroethane
60
144
35
64
139
35
NOTE: * Parameter outside of QC limits due to matrix effects.
Page 11
ORLANDO LABORATORIES, INC.
GC ORGANICS
MAT"R = X SP I KE RESULTS
MATRIX : SOIL/SEDIMENT/SOLIDS
REPORT DATE : 01-06-1992
LAB SAMPLE # 91-12-428-1
ANALYSIS DATE 1-5-92
AMOUNT SAMPLE MS MS % MSD MSD%
COMPOUND SPIKED RESULT RESULT RECOVERY RESULT RECOVERY RPD
NAPHTHALENE 88 0 62 78 58 73 7
FLUORENE 80 0 69 86 65 81 6
FLUORANTHENE 88 B 68 85 60 75 13
COMMENTS :
MATRIX SPIKE QUALITY CONTROL LIMITS
WATER SOIL
LOWER UPPER RPD LOWER UPPER RPD
NAPHTHALENE ; 55 126 28 ; 40 155 20
FLUORENE ; 30 128 20 30 155 20
FLUORANTHENE 53 150 20 35 150 28 ;
CODES
CFU Colony Forming Units
DIL Diluted Out
D.O. Diluted Out
H Greater Than 200 Background Colonies
J Indicates An Estimated Value
L Less Than 100 Background Colonies
M 100-200 Background Colonies
MCL Maximum Contaminant Level
N No Background Colonies
NA Not Applicable
N/C No Combustion
NR Not Requested
TNTC Too Numerous To Count
U Indicates the compound was analyzed for, but not detected. The numerical
value preceding 'U' is the limit of detection for that compound, based on
dilution.
< Less Than
> Greater Than
End of Report
11� vv�+vv
LANDO
P CG. Box 14oOrlando.
LABORATORIES, 328;4 CHAIN -OF -CUSTODY RECORD
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